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nmr_probes [2023/10/24 08:22] noji wish is now wish8.6 |
nmr_probes [2024/01/10 17:36] swartzj [Spectrograph NMR GUI "locks" in noise or does not see weak resonance] |
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===== Description ===== | ===== Description ===== | ||
- | The NMR running programs for both the S800 analysis line and spectrograph dipoles can be started by logging in to exp-s3-nmr.ftc (10.40.230.111) accessible from the EXP network, namely, from a whatever | + | The NMR running programs for both the S800 analysis line and spectrograph dipoles can be started by logging in to exp-s3-nmr.ftc (10.40.230.111) accessible from the EXP network, namely, from any computer connected to the EXP network, |
$ ssh [your-user-name-on-EXP]@exp-s3-nmr -Y | $ ssh [your-user-name-on-EXP]@exp-s3-nmr -Y | ||
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- | ==== Spectrograph | + | ==== NMR reading sometimes takes too long (> 30 min) ==== |
- | | + | |
- | * Threshold for the Spectrograph resonance | + | This is typically caused by one of two possible factors: |
+ | |||
+ | 1. The signal is weak, and so the NMR " | ||
+ | * This can be alleviated | ||
+ | * Stop NMR; enter new threshold (in Volts) and click “Set”; start NMR. | ||
+ | * In general, a threshold 0.15 mV is good for normal NMR signals, whereas 0.10 mV may be necessary if the signal are too weak. | ||
+ | |||
+ | 2. Initial field where NMR starts scanning is far away from actual value (this has only been seen with Spectrograph) | ||
+ | * Check what field is NMR scanning and compare with field read by neighboring NMR. | ||
+ | * If it is too far, stop NMR; enter field (in T) and click “Set”; start NMR. | ||
+ | |||