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nmr_probes [2019/10/14 00:28] pereira [Manually setting Dipole Fields] |
nmr_probes [2019/10/17 10:29] pereira [Manually setting Dipole Fields] |
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* Get access to the NMR controller in the mezzanine level of S3 vault (see figure below). Push the “SEARCH LOCAL” button to take control out of REMOTE mode. | * Get access to the NMR controller in the mezzanine level of S3 vault (see figure below). Push the “SEARCH LOCAL” button to take control out of REMOTE mode. | ||
* Select the right probe by turning the “probe knob” (see figure below). Remember, each dipole has two probes: probe 4, covers fields in the range 0.34 – 1.05 T, and probe 5 covers fields in the range 0.7–2.1 T. In this case, we should set the knob of the Spectrograph controller to position B | * Select the right probe by turning the “probe knob” (see figure below). Remember, each dipole has two probes: probe 4, covers fields in the range 0.34 – 1.05 T, and probe 5 covers fields in the range 0.7–2.1 T. In this case, we should set the knob of the Spectrograph controller to position B | ||
- | * The list of probes that can be selected with the knobs are, for the Spectrograph: | + | * The list of probes that can be selected with the knobs are, for the Spectrograph: |
* Use the “coarse” and “fine” knobs to select the field that you want (in T): 1.35454 T. By doing this, you are asking the NMR controller to just look at that field. | * Use the “coarse” and “fine” knobs to select the field that you want (in T): 1.35454 T. By doing this, you are asking the NMR controller to just look at that field. | ||
* If the field of that dipole happens to be close enough to the field that the NMR controller is looking at, Bingo! You’ll most likely see a resonance in the oscilloscope. In the most likely situation, however, your magnet is far away from the NMR search window and you will see only a flat line in the oscilloscope. | * If the field of that dipole happens to be close enough to the field that the NMR controller is looking at, Bingo! You’ll most likely see a resonance in the oscilloscope. In the most likely situation, however, your magnet is far away from the NMR search window and you will see only a flat line in the oscilloscope. |